天然产物研究与开发 ›› 2017, Vol. 29 ›› Issue (8): 1403-1408.doi: 10.16333/j.1001-6880.2017.8.024

• 开发研究 • 上一篇    下一篇

永州薄荷精油微波辅助提取工艺及具驱蚊功效空气清新剂研究

闫荣玲,廖阳*,王静,何福林*   

  1. 湖南科技学院 化学与生物工程学院 湘南优势植物资源综合利用省重点实验室,永州 425199
  • 出版日期:2017-08-28 发布日期:2017-08-28

Microwave-assisted Extraction of Essential Oil from Yongzhou Mentha haplocalyx and Formulation Development of Air Freshener with Mosquito Repelling Function

YAN Rong-ling,LIAO Yang*,WANG Jing,HE Fu-lin*   

  1. Key Laboratory of Comprehensive Utilization of Dominant Plant Resources in Southern Hunan,College of Life Sciences and Chemistry Engineering,Hunan University of Science and Engineering,Yongzhou 425199,China
  • Online:2017-08-28 Published:2017-08-28

摘要: 本文研究了永州薄荷精油的微波辅助提取工艺,并基于所得精油进行了植物源天然空气清新剂的研制。结果发现:(1)永州薄荷精油的最佳微波辅助水蒸气蒸馏提取工艺为料液比1:8、微波时间250 s、微波功率300 W、蒸馏时间2.5 h,在此最优条件下永州薄荷精油平均得率达3.3%;(2)基于薄荷精油与永州另一优势植物资源香姜精油复配研制植物源空气清新剂,发现基于二者的复方精油配方除臭效果优于各自的单方精油,且在二者配比为2:1(薄荷精油:香姜精油),总体积分数为6%时对臭气分子清除作用最佳,并表现出良好的趋蚊功效。结果表明,微波辅助可以获得较高的薄荷精油得率,所获精油搭配香姜精油开发多功能空气清新剂可行性强且效果好,研究结果可为永州地方优势植物资源综合利用提供参考。

关键词: 永州薄荷, 姜精油, 微波辅助, 水蒸气蒸馏, 空气清新剂

Abstract: In this study,microwave-assisted steam distillation extraction technology was developed and optimized for the extraction of essential oil from Yongzhou Mentha haplocalyx and a formulation of air refreshing agent with mosquito repelling function was developed.Results showed that,(1) the optimal extraction process of essential oil from Yongzhou M.haplocalyx were solid/liquid ratio of 1:8,microwave time of 250 s,microwave power of 300 W,distillation time of 2-5 h,the maximum yield of essential oil were 3.3% under the optimized conditions.(2) A air freshener was developed based on essential oil extracted from Yongzhou M.haplocalyx and R.zingiberis which was another local dominant plant resource,the formula showed the best performance of air freshing when the essential oil ratio was 2:1 (mint:ginger) and the total volume fraction of essential oil was 6%.In addition,it had an efficient and lasting mosquito repelling effect.The results indicated that,a higher extraction rate of essential oil from Yongzhou M.haplocalyx can be obtained by microwave-assisted extraction and the development of multi-functional air freshener based on the plant essential oil was feasible and effective.The results of this study can provide some reference for the comprehensive utilization of local plant resources in Yongzhou of Hunan province.

Key words: Yongzhou Mentha haplocalyx, essential oil, microwave assisted, steam distillation, air freshener