天然产物研究与开发 ›› 2015, Vol. 27 ›› Issue (12): 2060-2063.doi: 10.16333/j.1001-6880.2015.12.012

• 研究简报 • 上一篇    下一篇

壮药一匹绸根茎的化学成分

卢汝梅*,廖广凤,韦建华,李兵,林珍梅   

  1. 广西中医药大学药学院,南宁 530001
  • 出版日期:2015-12-29 发布日期:2016-01-06

Chemical Constituents in Roots and Rhizomes of Argyreia aceta

LU Ru-mei*,LIAO Guang-feng,WEI Jian-hua,LI Bing,LIN Zhen-mei   

  1. College of Pharmacy,Guangxi University of Chinese Medicine,Nanning 530001,China
  • Online:2015-12-29 Published:2016-01-06

摘要: 采用硅胶柱层析、Sephadex LH-20柱层析及HPLC色谱技术对壮药一匹绸根茎化学成份进行分离和纯化,从其石油醚部位和乙酸乙酯部位分离并鉴定了15个化合物,分别鉴定为东莨菪亭(1)、东莨菪苷(2)、橙黄胡椒酰胺(3)、N-反式-p-香豆酰基酪胺(4)、咖啡酸(5)、咖啡酸甲酯(6)、咖啡酸乙酯(7)、水杨酸(8)、3,7-二羟基-5,4′-二甲氧基黄酮(9)、木栓酮(10)、表木栓醇(11)、十六烷酸(12)、十六烷酸甘油酯(13)、β-谷甾醇(14)、胡萝卜苷(15)。其中,化合物1~13为首次从该植物中分离得到。

关键词: 一匹绸, 东莨菪亭, 东莨菪苷, 橙黄胡椒酰胺

Abstract: Fifteen compounds were isolated from EtOAc and n-BuOH extracts of roots and rhizomes of Zhuang Medicine Argyreia aceta Lour..On the basis of spectral data and literature,the isolated compounds were elucidated as scopoletin (1),scopolin (2),aurantiamide acetate (3),paprazine (4),caffeic acid (5),caffeic acid methyl ester (6),caffeic acid ethyl ester (7),salicylic acid (8),3,7-dihydroxy-5,4′-dimethoxyflavone (9),friedelin (10),epifriedelanol (11),n-hexadecanioc acid (12),1-O-hexadecanolenin (13),β-sitosterol (14) and daucosterol (15).Compounds 1-13 are isolated from A.aceta for the first time.

Key words: Argyreia aceta Lour., scopoletin, scopolin, aurantiamide acetate

中图分类号: 

R284.1