天然产物研究与开发 ›› 2016, Vol. 28 ›› Issue (Suppl1): 120-126.doi: 10.16333/j.10016880.2016.S.028

• 开发研究 • 上一篇    下一篇

优化超声盐溶辅助法艾纳香油提取工艺

张影波1,庞玉新1*,袁媛2,王丹1,胡璇1,王凯1,袁蕾1   

  1. 1中国热带农业科学院 热带作物品种资源研究所 海南省艾纳香工程技术研究中心,儋州 571737;2海南大学环境与植物保护学院,海口 570228
  • 出版日期:2016-06-30 发布日期:2017-03-02

Optimization of Ultrasonic and Saltingoutassisted Extraction of N lng Oil from Blumea balsamifera (L.) DC.(Asteraceae)

ZHANG Yingbo1,PANG Yuxin1*,YUAN Yuan2,WANG Dan1,HU Xuan1,WANG Kai1,YUAN Lei1   

  1. 1Tropical Crops Genetic Resources Institute;Hainan Provincial Engineering Research Center  for Blumea Balsamifera;Chinese Academy of Tropical Agricultural Sciences,Danzhou 571737,China; 2 Environment and Plant Protection College,Hainan University,Haikou 570228,China
  • Online:2016-06-30 Published:2017-03-02

摘要: 艾纳香油不仅被广泛应用于中药产业,其还是一种潜在的杀虫剂和防腐剂,水蒸气蒸馏法是一种高效、低成本获取艾纳香油的方法。本研究通过正交实验设计、优化超声时间、料夜比、盐溶辅助和提取时间来比较艾纳香油的提取率。艾纳香油最佳提取率为0.42%,最佳条件组合条件为超声时间为30 min、液料比为1:0.6、氯化钠质量分数为9.0%、提取时间为4.0 h。通过GCMS法分析艾纳香油的化学成分,鉴定出48中成分(9600%)。艾纳香油的主要成分为左旋龙脑(43.55%)、樟脑(9.54%)、1辛烯3醇(8.31%)、石竹烯(651%)、β蒎烯(5.20%)。

关键词: 艾纳香油, 艾纳香, 超声盐溶辅助水蒸馏, 提取工艺, 正交实验, 化学成分

Abstract: N lng [Blumea.balsamifera (L.) DC.] oil is one of the essential oil that has a wide variety of application in Chinese traditional medicine manufacturing industry,and also has a potential to be used as an insect repellent and antiseptic product in future.N lng oil is obtained using a steam distillation where an aromatic chemical is extracted from B.balsamifera (L.) DC.leaves by steam and condensed which provide relatively high yield of product and low cost of running the process.The aim of this study was to improve the yield of N lng oil extraction by using ultrasonicassisted,saltingoutassisted and optimizing the extraction condition.With the orthogonal test design,the ultrasonicassisted time,the ratio of of material to solvent,the concentration of sodium chloride and the time of extraction were compared to observe the effect on the extraction of volatile oil from N lng plants.The best N lng oil extraction rate by ultrasonicassisted saltingout hydrodistillation method was 0.42%,and the optimization combinations of best yield were when the ultrasonicassisted time was 30 min,the ratio of material to water was 1:06,the concentration of sodium chloride was 9.0% and extraction time was 4.0 h.The chemical compositions of N lng oil were also analyzed by GCMS,and 48 components (96.00%) were indentified.The dominant components in the N lng oil were borneol (43.55%),camphor (9.54%),1Octen3ol (8.31%),caryophyllene (6.51%) and βPinene (5.20%).

Key words: N lng oil, Blumea balsamifera (L.) DC., ultrasonicassisted saltingout hydrodistillation, extraction process, orthogonal test, chemical compositions

中图分类号: 

TQ35