天然产物研究与开发 ›› 2012, Vol. 23 ›› Issue (09): 1235-.doi: A

• 研究简报 • 上一篇    下一篇

维药香蜂花挥发油的GC-MS分析

杨 娟1,2，哈木拉提?吾甫尔1，赵鹤珊2，张 帆1,2*   

  1. 1新疆医科大学药学博士后流动站，乌鲁木齐 830011；2新疆名医名方与特色方剂重点实验室，乌鲁木齐 830011
  • 出版日期:2012-09-29 发布日期:2013-01-06
  • 基金资助:
    This research project was supported by the China Postdoctoral Science Foundation (No. 20100471678)

Analysis of Essential Oil Components in Melissa officinalis Linn by GC-MS

YANG Juan1, 2, Halmurat UPUR1, ZHAO He-shan2, ZHANG Fan1,2   

  1. 1Pharmaceutical Post-doctoral Station, Xinjiang Medical University, Urumqi 830011, China; 2Xinjiang Laboratory of Famous Prescription and Science of Formulas, Urumqi 830011, China
  • Online:2012-09-29 Published:2013-01-06

摘要： 结合气相色谱-质谱联用技术和保留指数对维医常用药材香蜂花挥发油提取物进行了分析。从该挥发油中共准确鉴定出28个化合物，占提取物总量的99.02%。结果发现，主要成分有(E)-3,7-dimethyl-2,6-octadien-1-ol acetate (26.48%)、(Z)-citral (15.46%)、(E)-nerol (14.51%)、(E)-citral (14.43%)、isoanisole (7.88%)、palmitic acid (6.93%)和(Z)-nerol (2.56%)，多为单萜和倍半萜类成分，为维药香蜂花的质量标准制定提供了科学依据。

关键词: 香蜂花, 挥发油, 气相色谱-质谱联用, 保留指数

Abstract: The essential oil components were analyzed in Melissa officinalis Linn by both GC-MS and retention indices at the same time. Essential oil obtained by hydrodistillation from dried aerial part of M. officinalis Linn collected from Xinjiang province (western China), was analyzed by gas chromatography-flame ionization detector (GC-FID), gas chromatography coupled to mass spectrometry (GC-MS) and all components’ retention indices. Twenty-eight constituents were accurately detected from the essential oil, accounting for 99.02% of the total amount. The quantitatively significant constituents of the essential oil were (E)-3,7-dimethyl-2,6-octadien-1-ol acetate (26.48%), (Z)-citral (15.46%), (E)-nerol (14.51%), (E)-citral (14.43%), isoanisole (7.88%), palmitic acid (6.93%) and (Z)-nerol (2.56%). The components of M. officinalis Linn essential oil were complicated and were dominated by mono- and sesquiterpene compounds, which were maybe the main biological activities.

Key words: Melissa officinalis Linn, essential oil, GC-MS, retention indices

中图分类号:  R284.1

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