NATURAL PRODUCT RESEARCH AND DEVELOPMENT ›› 2022, Vol. 34 ›› Issue (增刊1): 39-45.doi: 10.16333/j.1001-6880.2022.S.006

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Analysis of volatile components in Lavandula angustifolia Mill. by HS-SPME-GC-MS

CHEN Guo-tong1,2,MA Ping-ping1,MA Jin-lu3,YU Wen-jiao1,LI Mu-chun1,YANG Zhong1*   

  1. 1Xinjiang Academy of Analysis and Testing,Urumqi 830011,China;2College of Chemistry and Chemical Engineering,Xinjiang Normal University,Urumqi 830054,China; 3Institute for Pesticide Control of Xinjiang,Urumqi 830046,China
  • Online:2022-06-01 Published:2022-05-18

Abstract:

In order to obtain the volatile components of Lavandula angustifolia in natural state,the conditions of headspace solid phase micro-extraction gas chromatography-mass spectrometry (HS-SPME-GC-MS) were optimized by single factor test and orthogonal test.The volatile components of space blue,a representative variety of L. angustifolia,were analyzed at room temperature and compared with steam distillation (SD).The results showed that the optimum conditions of HS-SPME method were extraction time 60 min,equilibrium time 20 min and desorption time 5 min.Under this condition,34 chemical components were identified and 27 chemical components were identified by SD.The main compound types were acetate,alcohol and olefin compounds,among which linalool and linalyl acetate were the main compounds.The volatile components of L. angustifolia obtained by the two methods are quite different in both chemical composition and relative content.It provides a theoretical basis for rapid quality identification,quality evaluation and rational utilization of L. angustifolia varieties.

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